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Sinteze di-, tri- in polipeptidov na osnovi beta-heteroarilamino-alfa,beta-dehidro-alfa-amino kislin oziroma derivatov = The synthesys of di-, tri- in polypeptides from beta-heteroarylamino-alpha-beta-dehydro-alpha-amino acids and their derivatives
Aljaž-Rožič, Mateja
2-fenil-4-heteroarilaminometilen-%(4H)-oksazolone smo z aminokislinami v prisotnosti natrijevega karbonata pretvorili v ustrezne N-(2-benzoilamino-3-heteroarilaminopropenoil)-aminokisline. Le-te ...tvorijo z 2-kloro-4,6-dimetoksi-1,3,5-triazinom v prisotnosti N-metilmorfolina aktivirane estre, ki v naslednji stopnji reagirajo z estri aminokislin oziromapeptidov v ustrezne polipeptide. 2-fenil-4-heteroarilamino-metilen-5(4H)-oksazolone smo z dimetilformamidom dimetil acetalom N-metilirali. Nastali produkt se z aminokislinami v alkalnem ne odprejo, pač pa teče substitucija na beta-mastu glede na karbonilno skupino. Izolirali smo N-oksazolinil substituirane aminokisline
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