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  • Synthesis of Au nanoparticles prepared with ultrasonic spray pyrolysis and hydrogen reduction = Sinteza Au-nanodelcev, pripravljenih z ultrazvočno razpršilno pirolizo in redukcijo z vodikom
    Stopić, Srečko ...
    Golden nanoparticles of different sizes and shapes (spherical, cylindrical, triangular and round) where prepared during a synthesis of gold with ultrasonic spray pyrolysis (USP) and hydrogen ... reduction. The experimental investigations of the (USP) method were performed with an ultrasonic source of 0.8 MHz and 2.5 MHz, acting on the water solution of HAuCl4 forming aerosols with micron-sized and nanosized droplets. The results of the investigation show that the final shape and size of the Au particles depend on the characteristics of the solution and the frequency of the ultrasound. The second step of synthesizing the Au nanoparticles includes the subsequent thermal decomposition of the aerosol droplets in a hydrogen atmosphere between 260°C and 500°C. The investigations showed that the Au nanoparticles prepared in this way are smaller and more homogeneous.
    Source: Materiali in tehnologije = Materials and technology. - ISSN 1580-2949 (Letn. 47, št. 5, sep.-okt. 2013, str. 577-583)
    Type of material - article, component part
    Publish date - 2013
    Language - english
    COBISS.SI-ID - 17274390