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Four hybrid materials based on Preyssler ▫$P_5W_{30}$▫ polyoxometalate and first-row transition-metal complex
Hu, Tuo-Ping ...
Four Preyssler ▫$P_5W_{30}$▫ based inorganic-organic hybrids were synthesized hydrothermally. They exhibit different 3D networks ranging from ▫$(3,6)$▫-connected ant, pillared-layer, ...▫$(4,4)$▫-connected pts, and ▫$(5,5)$▫-connected ▫$\{4^5 \cdot 6^4 \cdot 8\}\{4^5 \cdot 6^5\}$▫ networks, respectively. The magnetism studies indicated antiferromagnetically coupled systems for the hexa- and pentanuclear Cu(II) units in 1 and 2, respectively. The electrochemical property demonstrates that all compounds have electrocatalytic abilities toward the reduction of hydrogen peroxide. Furthermore, the catalytic activities of 1 in the cyanosilylation of aldehydes reaction have been investigated.
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