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Sinteza in karakterizacija hidroksilamonijevega fluorosilikata in hidroksilamonijevega fluorogermanata
Ban, Irena ; Kristl, Matjaž ; Drofenik, Mihael
Sintetizirali smo novi spojini hidroksilamina, hidroksilamonijevfluorosilikat in hidroksilamonijevfluorogermanat. Spojine smo karakterizirali s kemijsko analizo, rentgenskimi praškovnimi posnetki in ...termično analizo. Pri razkroju hidroksilamonijevega fluorosilikata opazimo štiri endotermne pike; izguba mase pri 500 stopinjah celzije je blizu 100% zaradi sublimacije razkrojnih produktov. Hidroksilamonijevfluorogermanat razpade v štirih stopnjah, od katerih sta dva endotermna in dva eksotermna; končni produkt pri 500 stopinjah celzija je Germanijev oksid (IV).
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