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Sinteza in karakterizacija hidroksilamonijevega fluorokromata
Kristl, Matjaž ; Drofenik, Mihael ; Dimc, Franc
Raziskovali smo reakcije v sistemu CrF▫$_3$▫-NH▫$_3$▫OHF-HF-H▫$_2$▫O. Iz vodne raztopine smo izolirali zeleno mikrokristalinično fazo. Kemijska analiza je potrdila, da smo sintetizirali novo ...koordinacijsko spojino trivalentnega kroma s formulo (NH▫$_3$▫OH)▫$_3$▫CrF▫$_6$▫. Izmerili smo magnetno susceptibilnost spojine med 80 in 150 K. Podrobno smo preučili termični razkroj dobljene spojine, pri čemer smo preostanek karakterizirali z rentgenskimi praškovnimi posnetki.
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