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Preiskava mazalnih snovi iz WC/C prevlek na jeklu s spektroskopijo Augerjevih elektronov = AES analysis for identification of lubricating substances from diamond like WC/C coatings on steel
Hren, Denis ...
Preiskovali smo sestavo tribofilmov nastalih na jekleni površini. Tribofilme smo generirali iz prevleke diamantu podobnega ogljika, ki vsebuje volfram (WC/C), in sulfidne spojine raztopljene v ...polialfaolefinski osnovi (PAO). S spreminjanjem koncentracije sulfida v polialfaolefinu smo opazili spremembo triboloških lastnosti pri modelnih mehanskih preizkusih. Zato smo sklepali na različno sestavo generiranih triboloških plasti v mehanskem kontaktu. Najprej smo opravili več primerjalnih jedkanj na vseh tribološko generiranih površinah. Nato smo se zaradi nedvoumne primerjave plasti odločili za prirejeno tehniko jedkanja (variable sputtering time per cycle). Raziskavo smo opravili na visoko ločljivem SEM/AES/XPS sistemu s sferičnim energijskim analizatorjem in virom elektronov na poljsko emisijo (FE). V raziskanih plasteh smo lahko identificirali dve glavni vrsti spojin, katerih sestava se ujema z rezultati AES meritev.
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