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A carbonate-templated decanuclear Mn nanocage with two different silsesquioxane ligands
Sheng, Kai ...
The mild reaction of the preorganized silsesquioxane precursor with Mn(II) acetate under ambient conditions results in a mixed-valent ▫$\{ \mathrm{Mn^{II}_6 Mn^{III}_4}\}$▫ nanocage ...▫$\mathbf{(SD/Mn10)}$▫ which is protected by both acyclic trimer ▫$\mathrm{[Si3]}$▫ and cyclic tetramer ▫$\mathrm{[Si4]}$▫. Serendipitous capture of atmospheric ▫$\mathrm{CO_2}$▫ as a ▫$\mu_5$▫-carbonate anion placed at the center supports the formation of the cluster. The magnetic analysis reveals the strong antiferromagnetic interactions between Mn ions. Moreover, the dropcasting film of ▫$\mathbf{(SD/Mn10)}$▫ shows photoelectric activity indicating its great potential as a semiconductor for photoelectric conversion applications.
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