Synthesis of novel bicyclic nitroxides using partial Favorskii rearrangement
Babič, Andrej, 1979- ; Pečar, Slavko
3-bromo-2,2,6,6-tetramethyl-4-oxopiperidine-1-oxyl was reacted with several C-nucleophiles to give novel bicyclic pyrolidine nitroxides through partial Favorskii rearrangement.Further reduction with ...sodium borohydride gave spin probes with free hydroxyl groups and under harsh reduction conditions allowed the Favorskii rearrangement to proceed to completion
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