Obratovanje encimskega membranskega reaktorja pri superkritičnih pogojih
Primožič, Mateja, 1975- ; Leitgeb, Maja ; Knez, Željko
Razvili smo visokotlačni kontinuirani encimski membranski reaktor, v katerem smo uporabljali ultrafiltracijske membrane kot separacijsko enoto in kot reakcijski medij superkritične fIuide. Stabilnost ...membran pri visokih tlakih smo testirali na 3 različne načine. Po počasni ekspanziji smo določili hidrodinamske lastnosti in "MW cut-off' membrane, katere smo nato primerjali z lastnostmi originalne membrane. Na osnovi dobljenih rezultatov testiranja membran smo za encimsko kataJizirano reakcijo hidrolize sončničnega olja v visokotlačnem kontinuiranem encimskem membranskem reaktor ju uporabili polisulfonske in najlonske membrane, ki so bile uporabljene kot separacijski medij za ločitev encima od substratov in produktov pri večkratnih ponovitvah poizkusov. Reakcijo smo izvedli pri različnih pretokih substratov pri 50De in 200 bar ter kot katalizator uporabili lipazo Lipolase 100T.
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