Manganese-catalyzed synthesis of monofluoroalkenes via C-H activation and C-F cleavage

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Manganese-catalyzed synthesis of monofluoroalkenes via C-H activation and C-F cleavage

Cai, Sai-Hu; Ye, Lu; Wang, Ding-Xing; Wang, Yi-Qiu; Lai, Lin-Jie; Zhu, Chuan; Feng, Chao; Loh, Teck-Peng

Chemical communications (Cambridge, England), 2017, Volume: 53, Issue: 62

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The manganese-catalyzed α-fluoroalkenylation of arenes via C-H activation and C-F cleavage has been described. This protocol provides a very useful method for the synthesis of monofluoroalkenes with predominant unconventional E-isomer selectivity which complements the existing strategies for the access to these molecular architectures. In addition, the selectivity of β-defluorination in the catalytic cycle not only determines the configurations of the products but also obviates the use of external oxidants, providing a good example in the exploitation of manganese-catalyzed redox-neutral C-H transformations.

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