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Zhu, H.-Y; Fu, Y.-Q; Jiang, R; Jiang, J.-H; Xiao, L; Zeng, G.-M; Zhao, S.-L; Wang, Y
Chemical engineering journal (Lausanne, Switzerland : 1996), 09/2011, Volume: 173, Issue: 2Journal Article
Magnetic cellulose/Fe₃O₄/activated carbon composites (m-Cell/Fe₃O₄/ACCs) were prepared successfully and characterized by X-ray diffraction (XRD), Brunauer–Emmett–Teller (BET), thermogravimetric analysis (TGA), scanning electron microscopy (SEM) and vibrating sample magnetometer (VSM). The adsorption of congo red onto the novel m-Cell/Fe₃O₄/ACCs was studied as a function of contact time, initial concentration of congo red, adsorbent dosage, and pH of solution. The saturated magnetization of m-Cell/Fe₃O₄/ACCs reached 48.2emug⁻¹ and the magnetic adsorbent showed characteristics of superparamagnetism, which indicated that m-Cell/Fe₃O₄/ACCs could be separated from treated solution by a magnetic process. A comparison of kinetic models showed that the overall adsorption process was best described by pseudo-second-order kinetic model. Thermodynamic analysis indicated an exothermic nature of adsorption and a spontaneous and favorable process. The m-Cell/Fe₃O₄/ACCs might be a promising candidate of high efficiency, low cost and convenient separation under magnetic field.
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