Microwave-Assisted Hydrothermal Synthesis of Bi6(NO3)2O7(OH)2 and Its Photocatalytic Properties

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Microwave-Assisted Hydrothermal Synthesis of Bi6(NO3)2O7(OH)2 and Its Photocatalytic Properties

Egorysheva, A. V.; Gaitko, O. M.; Golodukhina, S. V.; Khoroshilov, A. V.; Fatyushina, E. V.; Dudkina, T. D.

Russian journal of inorganic chemistry, 2019/1, Volume: 64, Issue: 1

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Anhydrous basic bismuth nitrate Bi 6 (NO 3 ) 2 O 7 (OH) 2 was shown to be produced by reacting bismuth nitrate with aqueous ammonia under microwave-assisted hydrothermal treatment as a result of hydrolysis. The composition of the basic nitrate was verified by titration, CHNS analyses, DTG, and IR spectroscopy. Photocatalytic tests showed that Bi 6 (NO 3 ) 2 O 7 (OH) 2 has a photocatalytic activity, but its properties are interior to those of α-Bi 2 O 3 .

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