Synthesis of 2‑Sulfenylindenones via One-Pot Tandem Meyer–Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides

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Synthesis of 2‑Sulfenylindenones via One-Pot Tandem Meyer–Schuster Rearrangement and Radical Cyclization of Arylpropynols with Disulfides

Zhang, Xing-Song; Jiao, Jun-Ying; Zhang, Xiao-Hong; Hu, Bo-Lun; Zhang, Xing-Guo

Journal of organic chemistry, 07/2016, Volume: 81, Issue: 13

Journal Article

A tandem annulation of arylpropynols with disulfides has been developed for the synthesis of 2-sulfenylindenone derivatives. The reaction pathway involves one-pot tandem Meyer–Schuster rearrangement of arylpropynols and successive radical cyclization with disulfides. Various arylpropynols and disulfides with a number of functional groups are compatible in this reaction that affords the corresponding 2-sulfenylindenones in moderate to good yields.

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Zhang, Xing-Song | Jiao, Jun-Ying | Zhang, Xiao-Hong | Hu, Bo-Lun | Zhang, Xing-Guo

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