6π-Electrocyclization in water: microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones

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6π-Electrocyclization in water: microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones

Li, Xiao-Yun; Liu, Yan; Chen, Xiao-Lan; Lu, Xin-Yuan; Liang, Xing-Xing; Zhu, Shan-Shan; Wei, Chuan-Wan; Qu, Ling-Bo; Yu, Bing

Green chemistry : an international journal and green chemistry resource : GC, 07/2020, Volume: 22, Issue: 14

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Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives. The desired products were obtained in high yields through simple filtration. A remarkable E -factor of 0.45 and an EcoScale score of 85.5 were obtained. Microwave-assisted synthesis of polyheterocyclic-fused quinoline-2-thiones through the annulation of ortho -heteroaryl anilines and CS 2 was realized in water without using any catalysts and additives.

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