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Prikhna, T.; Eisterer, M.; Gawalek, W.; Kozyrev, A.; Weber, H. W.; Sokolovsky, V.; Chaud, X.; Noudem, J.; Habisreuther, T.; Moshchil, V.; Karpets, M.; Basyuk, T.; Kovylaev, V.; Dellith, J.; Sverdun, V.; Kuznietsov, R.; Shmidt, C.; Vitovetskaya, T.; Polikarpova, L.
Journal of superconductivity and novel magnetism, 05/2013, Volume: 26, Issue: 5Journal Article
The volume pinning force, F p(max) , increases with increasing synthesis or sintering pressure (0.1 MPa–2 GPa) in materials prepared at high temperature (1050 °C) while it stays practically unchanged in those prepared at low temperature (800 °C). The position of F p(max) can be shifted to higher magnetic fields by: (1) increasing the manufacturing pressure or decreasing the temperature (2) additions (Ti, SiC, or C, for example), and (3) in-situ preparation. Grain boundary pinning (GBP) dominates in materials prepared at low temperatures (600–800 °C), while high-temperature preparation induces strong point pinning (PP) or mixed pinning (MP) leading to outstanding properties. In materials produced by spark plasma sintering (SPS), the position of F p(max) is higher than expected for both grain boundary and point pinning. The distribution of boron and oxygen in MgB 2 based material, which can changed by additions or the preparation conditions, significantly affects the type and strength of pining. Materials prepared under a pressure of 2 GPa with a nominal composition of Mg:7B or Mg:12B consist of 88.5 wt % MgB 12 , 2.5 wt % MgB 2 , 9 wt % MgO or 53 wt % MgB 12 , 31 wt % MgB 20 16 wt % MgO, respectively. Their magnetic shielding fractions at low temperatures are 10 % and 1.5 %, with a transition temperature, T c of 37.4–37.6 K. Although their magnetic critical current density at zero field and 20 K was 2–5×10 2 A/cm 2 , they were found to be insulating on the macroscopic level.
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