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Zhang, Tian-Shu; Hao, Wen-Juan; Wang, Rong; Wang, Shi-Chao; Tu, Shu-Jiang; Jiang, Bo
Green chemistry : an international journal and green chemistry resource : GC, 07/2020, Volume: 22, Issue: 13Journal Article
A new electrochemically induced three-component annulation-halosulfonylation of 1,6-enynes has been developed for stereoselective synthesis of 33 examples of 1-indanones with generally good yields under environmentally benign conditions. This electrochemical strategy can proceed in a simple undivided cell, avoiding any transition metal catalysts, chemical oxidants and additives. This reaction tolerates a wide scope of substrates, which provides a new and green access to fabricate important bioactive 1-indanone scaffolds. Notably, readily available and low-cost halogen salts play triple roles of an electrolyte and a redox catalyst as well as a halogenating reagent. A new electrochemically induced three-component annulation-halosulfonylation of 1,6-enynes has been developed for stereoselective synthesis of 33 examples of 1-indanones with generally good yields under environmentally benign conditions.
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