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Zhao, Jie; Li, Zi-Yu; Yang, Chun-Xu; Li, Ya-Ping; Liu, Yu-Shen; Hu, Zhen Hua; Pan, Xiao-Ming; Ma, Xiu-Li; Wang, Wei; Yang, Xiao-Shuai; Wang, Lu-Liang
Journal of the science of food and agriculture, 01/2024, Volume: 104, Issue: 1Journal Article
Phenolic endocrine-disrupting chemicals (EDCs) are widespread and easily ingested through the food chain. They pose a serious threat to human health. Magnetic solid-phase extraction (MSPE) is an effective sample pre-treatment technology to determine traces of phenolic EDCs. Magnetic covalent organic framework (COF) (Fe O @COF) nanospheres were prepared and characterized. The efficient and selective extraction of phenolic EDCs relies on a large specific surface and the inherent porosity of COFs and hydrogen bonding, π-π, and hydrophobic interactions between COF shells and phenolic EDCs. Under optimal conditions, the proposed magnetic solid-phase extraction-high-performance liquid chromatography-ultra violet (MSPE-HPLC-UV) based on the metallic covalent organic framework method for phenolic EDCs shows good linearities (0.002-6 μg mL ), with R of 0.995 or higher, and low limits of detection (6-1.200 ng mL ). Magnetic covalent organic frameworks (Fe O @COFs) with good MSPE performance for phenolic EDCs were synthesized by the solvothermal method. The magnetic covalent organic framework-based MSPE-HPLC-UV method was applied successfully to determine phenolic EDCs in beverage and water samples with satisfactory recoveries (90.200%-123%) and relative standard deviations (2.100%-12.100%). © 2023 Society of Chemical Industry.
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