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Yang, Jun; Ji, Ding-Wei; Hu, Yan-Cheng; Min, Xiang-Ting; Zhou, Xiangge; Chen, Qing-An
Chemical science, 11/2019, Volume: 1, Issue: 41Journal Article
Terpenes, consisting of isoprene monomer units, represent a family of naturally abundant compounds. The difunctionalization of terpenes is highly appealing yet remains challenging, since the multiple unbiased C&z.dbd;C bonds of terpenes lead to difficulty in controlling the regioselectivity. Herein, a cobalt( iii )-catalyzed C-H activation strategy has been developed to facilitate hydroxymethylarylation of terpenes with formaldehyde and arenes with high chemo- and regio-selectivities. These (chemo- and regio-) selectivities are governed by the coordination abilities of isoprene, directing groups and the steric effect. This terpene difunctionalization also features high atom and step economy through a C-H addition pathway. A cobalt( iii )-catalyzed C-H activation strategy has been developed to facilitate hydroxymethylarylation of terpenes with formaldehyde and arenes with high chemo- and regio-selectivities.
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