Copper-Catalyzed Tandem Trifluoromethylation/Semipinacol Rearrangement of Allylic Alcohols

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Copper-Catalyzed Tandem Trifluoromethylation/Semipinacol Rearrangement of Allylic Alcohols

Chen, Zhi-Min; Bai, Wei; Wang, Shao-Hua; Yang, Bin-Miao; Tu, Yong-Qiang; Zhang, Fu-Min

Angewandte Chemie (International ed.), September 9, 2013, Volume: 52, Issue: 37

Journal Article

Tandem jump: A novel copper‐catalyzed tandem trifluoromethylation/semipinacol rearrangement reaction of allylic alcohols has been achieved under mild conditions. This reaction is valuable for the difunctionalization of alkenes through simultaneous construction of a C sp 3CF3 bond and a quaternary carbon center, and could provide a straightforward strategy for the preparation of α‐quaternary β‐trifluoromethyl ketone derivatives.

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