De Novo Synthesis of γ,γ-Disubstituted Butyrolactones through a Visible Light Photocatalytic Arylation-Lactonization Sequence

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De Novo Synthesis of γ,γ-Disubstituted Butyrolactones through a Visible Light Photocatalytic Arylation-Lactonization Sequence

Guo, Wei; Cheng, Hong-Gang; Chen, Li-Yan; Xuan, Jun; Feng, Zhu-Jia; Chen, Jia-Rong; Lu, Liang-Qiu; Xiao, Wen-Jing

Advanced synthesis & catalysis, September 15, 2014, Volume: 356, Issue: 13

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A visible light photocatalytic arylation–lactonization sequence has been developed for the synthesis of γ,γ‐disubstituted butyrolactones. This unprecedented transformation features simple experimental procedures under very mild conditions. A one‐step synthesis of isobenzofuran‐1(3H)‐one has been carried out to demonstrate the synthetic application of this reaction.

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