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Jian, Xiao-Dong; Lu, Biao; Li, Dan-Dan; Yao, Ying-Bang; Tao, Tao; Liang, Bo; Guo, Jin-Hong; Zeng, Yi-Jiang; Chen, Jia-Le; Lu, Sheng-Guo
ACS applied materials & interfaces, 02/2018, Letnik: 10, Številka: 5Journal Article
Barium zirconate titanate (BZT) (Ba(Zr x Ti1–x )O3) ceramics with Zr4+ contents of x = 5, 10, 15, 20, 25, and 30 mol % were prepared using a solid-state reaction approach. The microstructures, morphologies, and electric properties were characterized using X-ray diffraction, scanning electron microscopy, and impedance analysis methods, respectively. The dielectric analyses indicate that the BZT bulk ceramics show characteristics of phase transition from a normal ferroelectric to a relaxor ferroelectric with the increasing Zr4+ ionic content. The electrocaloric effect adiabatic temperature change decreases with the increasing Zr4+ content. The highest adiabatic temperature change obtained is 2.4 K for BZT ceramics with a 5 mol % of Zr4+ ionic content.
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