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Guselnikova, Olga; Marque, Sylvain R. A; Tretyakov, Evgeny V; Mares, David; Jerabek, Vitezslav; Audran, Gérard; Joly, Jean-Patrick; Trusova, Marina; Svorcik, Vaclav; Lyutakov, Oleksiy; Postnikov, Pavel
Journal of materials chemistry. A, Materials for energy and sustainability, 2019, Letnik: 7, Številka: 2Journal Article
A plasmon as a stimulus opens up new opportunities for selective and regulated "from-surface" polymerization and functionalization of surfaces. Here, the first example of plasmon-assisted nitroxide-mediated polymerization (NMP) of stimuli-responsive block copolymers poly( N -isopropylacrylamide)- co -4-vinylboronic acid is reported. The growth of a polymer film at room temperature was achieved via plasmon-induced homolysis of alkoxyamines covalently attached to the surface of plasmon-active gold gratings at room temperature. Control of temperature, finite-difference time-domain method simulation of plasmon intensity distribution shift during polymerization, electron paramagnetic resonance experiments and other assays provide strong support for the plasmon-initiated mechanism of NMP. We demonstrated not only the control of the resulting polymer thickness but also the preparation of a surface-enhanced Raman spectroscopy chip for the detection of glycoproteins as a powerful example of plasmon-assisted NMP potential. The first method of plasmon-induced nitroxide-mediated polymerization on periodical gold gratings has been developed.
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