Production of density gradient aerogels with predetermined density steps or gradient is challenging, particularly when the experiments would demand a prescribed gradient in density along the axis of cylindrical shaped aerogel. In order to achieve this, it is vital to characterize and accurately measure the density gradient in order to “design” synthetic routes to achieve the desired density gradient that can be used in plasma physics experiments using high-energy lasers. X-ray tomography was used for the characterization of these aerogels and it is demonstrated that it is the most reliable and quick method for characterization of gradient density aerogels. Divinyl benzene aerogels samples were synthesized by Lewis acid catalysis and samples were supercritically dried, characterized and their parameters measured to realize that the necessary properties were achieved. The change in density from solid density to 100 mg/cm 3 is registered and the accuracy is evaluated.