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Hsu, Chun-Han; Pan, Zheng-Bang; Qu, Hau-Ting; Chen, Chuan-Ren; Lin, Hong-Ping; Sun, I-Wen; Huang, Ching-Ying; Li, Chun-Han
RSC advances, 04/2021, Letnik: 11, Številka: 26Journal Article
A green synthesis method is proposed for the preparation of nitrogen-doped multiporous carbons (denoted as N-MPCs) from water-caltrop shell (WCS) using eggshell waste as both a nitrogen-dopant and an activating agent. It is shown that the surface area, porosity, yield and nitrogen content of the as-prepared N-MPCs can be easily controlled by adjusting the activation temperature. Moreover, in oxygen reduction reaction (ORR) tests performed in O 2 -saturated 0.1 M KOH (aq) electrolyte containing 1.0 M methanol, the N-MPC catalysts show a high ORR stability and good resistance to methanol corrosion. In addition, as a cathode material in Al-air battery tests, the N-MPCs achieve a power density of 16 mW g −1 in a saturated NaCl (aq) electrolyte. Overall, the results show that the N-MPCs have a promising potential as a green and sustainable material for ORR catalysis applications. A green synthetic method is proposed for the preparation of nitrogen-doped multiporous carbons (denoted as N-MPCs) from water-caltrop-shell (WCS) biochar by using eggshell waste as both a nitrogen-dopant and an activating agent.
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in: SICRIS
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