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Louie, Shayan; Zhong, Yu; Bao, Si Tong; Schaack, Cedric; Montoya, Alvaro; Jin, Zexin; Orchanian, Nicholas M.; Liu, Yang; Lei, Wenrui; Harrison, Kelsey; Hone, James; Angerhofer, Alexander; Evans, Austin M.; Nuckolls, Colin P.
Journal of the American Chemical Society, 03/2023, Letnik: 145, Številka: 9Journal Article
Here, we describe the synthesis of the hexameric macrocyclic aniline (MA6), which spontaneously assembles into coaxially conductive organic wires in its oxidized and acidified emeraldine salt (ES) form. Electrical measurements reveal that ES-MA6 exhibits high electrical conductivity (7.5 × 10–2 S·cm–1) and that this conductivity is acid–base responsive. Single-crystal X-ray crystallography reveals that ES-MA6 assembles into well-defined trimeric units that then stack into nanotubes with regular channels, providing a potential route to synthetic nanotubes that are leveraged for ion or small molecule transport. Ultraviolet–visible–near-infrared absorbance spectroscopy and electron paramagnetic spectroscopy showcase the interconversion between acidic (conductive) and basic (insulating) forms of these macrocycles and how charge carriers are formed through protonation, giving rise to the experimentally observed high electrical conductivity.
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in: SICRIS
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