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Llansola Portolés, Manuel J; Pis Diez, Reinaldo; Dell’Arciprete, María L; Caregnato, Paula; Romero, Juan José; Mártire, Daniel O; Azzaroni, Omar; Ceolín, Marcelo; Gonzalez, Mónica C
Journal of physical chemistry. C, 05/2012, Letnik: 116, Številka: 20Journal Article
Silicon nanoparticles of 1–5 nm size (SiNPs) were synthesized by a bottom-up (BU) approach involving a chemical wet method. The contribution of different emitters to the overall excitation–emission matrix was analyzed on the assumption that pure substances existing in a unique form show an excitation wavelength-invariant emission spectrum. The occurrence of emitters differing in size and aggregation was supported by transmission electron microscopy (TEM), small-angle X-ray scattering (SAXS), time-resolved single photon counting, and time-resolved anisotropy experiments. The effect on photoluminescence (PL) of the particle surface oxidation as a result of aging is studied and compared to that of surface oxidized particles obtained by a top-down (TD) approach following an electrochemical method with HF etching. Surface oxidation to SiO x seems to introduce two different effects on the SiNP PL. An emission originated in surface states associated to SiO x was identified and observed for SiNPs synthesized by both BU and TD approaches. Blue-shifted excitation–emission spectra associated to a silicon core in embedded SiO x nanostructures were also identified. Theoretical studies were carried out to help understand the observed results.
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JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
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Vir: Osebne bibliografije
in: SICRIS
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