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Pericas, Miquel A; Herrerias, Clara I; Sola, Lluis
Advanced synthesis & catalysis, April 7, 2008, Letnik: 350, Številka: 6Journal Article
A functional polymer 4, obtained by reaction of (R)‐2‐(1‐piperazinyl)‐1,1,2‐triphenylethanol with a Merrifield resin, has been loaded in a packed bed reactor and used as catalyst for the continuous enantioselective production of 1‐arylpropanols by ethylation of aromatic aldehydes. The high catalytic activity depicted by 4 allows the complete conversion of the substrates with the use of stoichiometric reagent ratios and unprecedently short residence times (down to 2.8 min). In practice, a single‐pass operation can be used for all the studied aldehydes, and productions of up to 13.0 mol/g h are recorded. The sequential operation of the flow system for the uninterrupted synthesis of a small library of enantiopure 1‐arylpropanols is also reported.
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