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Kagan, Benjamin D.; Lichtscheidl, Alejandro G.; Erickson, Karla A.; Monreal, Marisa J.; Scott, Brian L.; Nelson, Andrew T.; Kiplinger, Jaqueline L.
European journal of inorganic chemistry, March 22, 2018, Letnik: 2018, Številka: 11Journal Article
Trimethyltin fluoride (Me3SnF) is a mild and selective reagent for the installation of actinide fluoride bonds as demonstrated by the room temperature synthesis of a variety of organometallic and inorganic thorium(IV), uranium(IV), and uranium(V) fluoride complexes {(1,2,4‐tBu3C5H2)2ThF2, (C5Me5)2U(F)(O‐2,6‐iPr2C6H3), U(F)(O‐2,6‐tBu2C6H3)3, U(F)N(SiMe3)23, (C5Me5)2UF2(L) (L = O=PMe3, O=PPh3, O=PCy3), and (C5Me5)2U(F)(=N‐2,6‐iPr2C6H3)} from their corresponding chloride, bromide, and iodide analogues. From these reactions, the new (C5Me5)2UF2(L) (L = O=PPh3, O=PCy3) uranium fluoride complexes were isolated and characterized by NMR spectroscopy and X‐ray crystallography. Trimethyltin fluoride (Me3SnF) is a mild and selective reagent for the installation of actinide fluoride bonds as demonstrated by the room temperature synthesis of a variety of organometallic and inorganic thorium and uranium from their corresponding chloride, bromide, and iodide analogues.
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in: SICRIS
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