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Papachlimitzou, Alexandra; Barber, Jonathan L.; Losada, Sara; Bersuder, Philippe; Law, Robin J.
Journal of Chromatography A, 01/2012, Letnik: 1219, Številka: 6Journal Article
► Analytical methodologies for the determination of NBFRs were reviewed. ► Considerable variations exist between methods used in different studies. ► Reported methods frequently lack the detail necessary to assess their quality. ► Quality of methods needs to be assessed using interlaboratory comparison exercises. ► Improvement would come with the use of reference materials and labelled standards. This review provides a summary of various analytical methodologies applied to the determination of “novel” brominated flame retardants (NBFRs) in various environmental compartments, as reported in peer reviewed literature, either in print or online, until the end of 2010. NBFRs are defined here as those brominated flame retardants (BFRs) which are either new to the market or newly/recently observed in the environment. The preparation and extraction of sediment, water, sewage sludge, soil, air and marine biota samples, the extract clean-up/fractionation and subsequent instrumental analysis of NBFRs are described and critically examined. Generally, while the instrumental analysis step mainly relies on mass-spectrometric detection specifically developed for NBFRs, and hyphenated to liquid or gas chromatography, preceding steps tend to replicate methodologies applied to the determination of traditional BFRs such as polybrominated diphenyl ethers (PBDEs) and hexabromocyclododecane (HBCD). Shortcomings and gaps are discussed and recommendations for future development are given.
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