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Zhang, Mingjie; Han, Chen; Chen, Wenyao; Luo, Wei; Cao, Yueqiang; Qian, Gang; Zhou, Xinggui; Duan, Xiaoguang; Wang, Shaobin; Duan, Xuezhi
Green energy & environment, October 2020, 2020-10-00, 2020-10-01, Letnik: 5, Številka: 4Journal Article
Heteroatom-doping of carbocatalysts has been a powerful strategy to remarkably enhance the catalytic performance. Herein, the underlying nature of N promotional effects on peroxymonosulfate (PMS) activation for phenol removal is understood by combining kinetics analysis with multiple techniques. A strategy using mixed acid oxidation of carbon nanotube (CNT) followed by NH3 treatment is employed to yield a series of catalysts with different N-doping contents but similar fraction of sp2-hybridized carbon and defective degree, endowing with a chance to discriminate the dominant N-containing active sites. The multi-sites kinetics analysis suggests the graphitic N-containing sites as the dominant active sites. The mechanism of the surface-bound reactive species is also discriminated as the dominant reaction mechanism. The insights reported here could provide the methodology to fundamentally understand the heteroatom-doping effects of carbocatalysis. Display omitted
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