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Dutta, Shanta; Yu, Iris K.M.; Tsang, Daniel C.W.; Su, Zhishan; Hu, Changwei; Wu, Kevin C.W.; Yip, Alex C.K.; Ok, Yong Sik; Poon, Chi Sun
Bioresource technology, February 2020, 2020-Feb, 2020-02-00, 20200201, Letnik: 298Journal Article
Display omitted •Green co-solvent systems enhanced cellulose depolymerization and product yield.•Maximum 32% of levulinic acid (LA) yielded in GVL/H2O solvent at 200 °C.•GVL/H2O system maintained high availability of soluble sugars.•Acetone/H2O solvent generated 17 Cmol% of LA at a lower temperature (180 °C)•Higher temperature induced polymerization of sugars in acetone/H2O solvent. Lignocellulosic wastes constitute a significant portion of the municipal solid waste, which should be valorised for the synthesis of value-added chemicals to achieve circular bioeconomy. This study evaluates the use of γ-valerolactone (GVL) and acetone as green co-solvents to produce levulinic acid (LA) from lignocellulosic paper towel waste at different temperatures using dilute H2SO4. At the highest reaction temperature (200 °C), H2O-only system achieved ~15 Cmol% of LA at maximum. while GVL/H2O and acetone/H2O co-solvent systems enhanced the depolymerisation of paper towel waste and the subsequent conversion to LA, with the highest yield amounted to ~32 Cmol%. Acetone/H2O solvent system generated ~17 Cmol% LA at a lower temperature (180 °C), while higher temperature induced polymerisation of soluble sugars and intermediates, hindering further conversion to LA. In contrast, the availability of soluble sugars was higher in the GVL/H2O system, which favoured the production of LA at higher temperatures.
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