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Domain size distribution of Y-TZP nano-particles using XRD and HRTEMBoulc'h, Florence ...Yttria doped nanocrystalline zirconia powder was prepared by spray-pyrolysis technique. Powder crystallized into tetragonal form, as dense and compositionally homogeneous polycrystalline spheres. ... X-Ray diffraction (XRD) and high resolution transmission electron microscopy (HRTEM) have been used inorder to characterize the mean size and the size distribution of crystallinedomains. An average size of 6 nm was calculated by Scherrer formulafrom X-Ray diffraction pattern. The domain size, determined by analysismethod developed by Hytch from HRTEM observations, ranges from 5 to 22nm with a main population around the value 12 nm. Limits and complementary nature of XRD and HRTEM methods are discussed.Source: Image analysis & stereology : official journal of the International Society for Stereology. - ISSN 1580-3139 (Vol. 20, no. 3, nov. 2001, str. 157-161)Type of material - article, component partPublish date - 2001Language - englishCOBISS.SI-ID - 16036057
Author
Boulc'h, Florence |
Schoulder, Marie-Claude |
Donnadieu, Patricia |
Chaix, Jean-Marc |
Djurado, Elisabeth
Topics
Particle Size |
X-Ray Diffraction |
Microscopy, Electron |
Image Processing, Computer-Assisted |
Crystallization |
Zirconium |
Yttrium |
Delec, velikost |
Mikroskopija elektronska |
Rentgenski žarki, lomljenje |
Slika, obdelava z računalnikom |
Cirkonij |
Itrij |
Kristalizacija |
kristalizacija |
cirkonij |
itrij |
analiza slik |
elektronska mikroskopija |
metode
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source: Image analysis & stereology : official journal of the International Society for Stereology. - ISSN 1580-3139 (Vol. 20, no. 3, nov. 2001, str. 157-161)
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Boulc'h, Florence | ![]() |
Schoulder, Marie-Claude | ![]() |
Donnadieu, Patricia | ![]() |
Chaix, Jean-Marc | ![]() |
Djurado, Elisabeth | ![]() |
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