AgNTf 2 -Catalyzed Regioselective C-H Alkenylation of N,N -Dialkylanilines with Ynamides

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AgNTf 2 -Catalyzed Regioselective C-H Alkenylation of N,N -Dialkylanilines with Ynamides

Nie, Xiao-Di; Mao, Zhuo-Ya; Guo, Jia-Ming; Si, Chang-Mei; Wei, Bang-Guo; Lin, Guo-Qiang

Journal of organic chemistry, 03/2022, Volume: 87, Issue: 5

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Regioselective C-H alkenylation of -dialkylanilines with ynamides was developed using AgNTf as a catalyst. This approach represents a facile hydroarylation of ynamides, allowing for the introduction of an alkenyl group exclusively at the position of aniline derivatives. As a result, a series of 4-alkenyl -dialkylanilines were synthesized with excellent regioselectivities.

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