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McCormack, Scott J.; Tseng, Kuo‐Pin; Weber, Richard J. K.; Kapush, Denys; Ushakov, Sergey V.; Navrotsky, Alexandra; Kriven, Waltraud M.
Journal of the American Ceramic Society, 08/2019, Volume: 102, Issue: 8Journal Article
Abstract The previously unknown experimental HfO 2 –Ta 2 O 5 ‐temperature phase diagram has been elucidated up to 3000°C using a quadrupole lamp furnace and conical nozzle levitator system equipped with a CO 2 laser, in conjunction with synchrotron X‐ray diffraction. These in‐situ techniques allowed the determination of the following: (a) liquidus, solidus, and invariant transformation temperatures as a function of composition from thermal arrest experiments, (b) determination of equilibrium phases through testing of reversibility via in‐situ X‐ray diffraction, and (c) molar volume measurements as a function of temperature for equilibrium phases. From these, an experimental HfO 2 –Ta 2 O 5 ‐temperature phase diagram has been constructed which is consistent with the Gibbs Phase Rule.
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