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Hu, Yulin; Yang, Lili; Liu, Xiaobing
Molecules (Basel, Switzerland), 12/2022, Volume: 28, Issue: 1Journal Article
A type of MCM-41 supported dicationic imidazolium ionic liquid nanocatalyst has been synthesized and found to be competent for the synthesis of 2-oxazolidinones through the sustainable chemical conversion of CO with aziridines. It was shown that the highest efficiency was achieved in the cycloaddition of a series of aziridines and CO in the presence of a catalytic amount of the solid catalyst MCM-41@ILLaCl under mild conditions. Merits of this meticulously designed protocol are the use of a novel supported ionic liquid catalyst, the easy work-up process, good to excellent yields, a short reaction time, and purification without column chromatography. Overall, the present protocol of synthesizing 2-oxazolidinones under cocatalyst- and solvent-free conditions using MCM-41@ILLaCl is promising for industrial applications.
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