Purpose
To evaluate and compare the mechanical properties (flexural strength and surface hardness) of different materials and technologies for denture base fabrication. The study emphasized the ...digital technologies of computer‐aided design/computer‐aided manufacturing (CAD/CAM) and three‐dimensional (3D) printing.
Materials and Methods
A total of 160 rectangular specimens were fabricated from three conventional heat‐polymerized (ProBase Hot, Paladon 65, and Interacryl Hot), three CAD/CAM produced (IvoBase CAD, Interdent CC disc PMMA, and Polident CAD/CAM disc), one 3D‐printed (NextDent Base), and one polyamide material (Vertex ThermoSens) for denture base fabrication. The flexural strength test was the three‐point flexure test, while hardness testing was conducted using the Brinell method. The data were analyzed using descriptive and analytical statistics (α = 0.05).
Results
During flexural testing, the IvoBase CAD and Vertex ThermoSens specimens did not fracture during loading. The flexural strength values of the other groups ranged from 71.7 ± 7.4 MPa to 111.9 ± 4.3 MPa. The surface hardness values ranged from 67.13 ± 10.64 MPa to 145.66 ± 2.22 MPa. There were significant differences between the tested materials for both flexural strength and surface hardness. There were also differences between some materials with the same polymerization type. CAD/CAM and polyamide materials had the highest flexural strength values. Two groups of CAD/CAM materials had the highest surface hardness values, while a third, along with the polyamide material, had the lowest. The 3D‐printed materials had the lowest flexural strength values.
Conclusions
Generally, CAD/CAM materials show better mechanical properties than heat‐polymerized and 3D‐printed acrylics do. Nevertheless, a material's polymerization type is no guarantee of its optimal mechanical properties.
This study aimed to determine the effects of three different varnish materials (containing casein phosphopeptide-amorphous calcium phosphate, nano-hydroxyapatite, and fluoride) on enamel. ...Thirty-three extracted human third molars were used for specimen preparation. These were demineralized using phosphoric acid. Three experimental groups (n = 11) were treated with 3M™ Clinpro™ White Varnish, MI Varnish®, and Megasonex® toothpaste, respectively, every twenty-four hours for fourteen days. Analysis of the microhardness of the specimens’ enamel surfaces was carried out via the Vickers method, and by scanning electron microscopy/energy dispersive X-ray spectroscopy (SEM/EDS). Analysis was performed at three stages: at baseline value, after demineralization, and after the period of remineralization. Data were subjected to Scheffe’s post hoc test. The mean microhardness values (HV0.1) obtained for the group of samples treated with MI Varnish® were higher compared with the other two groups (p = 0.001 for both comparisons), while the first and third groups did not differ significantly from each other (p = 0.97). SEM analysis showed uneven patterns and porosities on all samples tested. EDS results showed an increase in the mineral content of the examined samples, with the highest mineral content observed in the MI Varnish® group. It can be concluded that MI Varnish® use has a better remineralization effect on enamel than the other two materials.
With the emergence of digital technologies, new materials have become available for occlusal devices. However, data are scarce about these different materials and technologies and their mechanical ...properties.
The purpose of this in vitro study was to investigate the flexural strength and surface hardness of different materials using different technologies for occlusal device fabrication, with an emphasis on the digital technologies of computer-aided design and computer-aided manufacturing (CAD-CAM) and 3D printing.
A total of 140 rectangular specimens were fabricated from two 3D-printed (VarseoWax Splint and Ortho Rigid), 2 CAD-CAM–produced (Ceramill Splintec and CopraDur), and 3 conventional autopolymerizing occlusal device materials (ProBase Cold, Resilit S, and Orthocryl) according to ISO 20795-1:2013. Flexural strength and surface hardness were determined for 10 specimens of each tested material using the 3-point bend test and the Brinell method. The data were analyzed using descriptive statistics and 1-way ANOVA with Bonferroni corrections (α=.05).
Surface hardness values ranged from 28.5 ±2.5 MPa to 116.2 ±1.6 MPa. During flexural testing, neither the CopraDur nor the VarseoWax Splint specimens fractured during loading within the end limits of the penetrant’s possible movement. Flexural strength values for other groups ranged from 75.0 ±12.0 MPa to 104.9 ±6.2 MPa. Statistical analysis determined significant differences among the tested materials for flexural strength and surface hardness.
Mechanical properties among different occlusal device materials were significantly different. Acrylic resins were less flexible than polyamide and nonacrylic occlusal device materials for 3D printing but had higher and more consistent values of surface hardness. Clinicians should consider the different mechanical properties of the available materials when choosing occlusal device materials.
Silanized glass fibers are popular reinforcements of acrylic denture base materials. To increase the number of surface hydroxyl groups and to improve interfacial adhesion between the matrix and ...reinforcements, acid or base treatments of glass fibers are commonly performed before the silanization. However, limited data are available on the effect of these treatments on the mechanical properties of acrylic matrix composite materials used for denture base applications. In this work, before the silanization of a woven glass fiber fabric (GF) with 3-(trimethoxysilyl) propyl methacrylate, activation pretreatments using HCl and NH
OH aqueous solutions have been performed. To characterize the glass surface, FTIR spectroscopy was used. Specimens of cured acrylic denture base resin and composites were divided into five groups: (1) cured acrylic denture base resin-control group; (2) composite with non-silanized GF; (3) composite with silanized GF; (4) composite with NH
OH activated and silanized GF; (5) composite with HCl activated and silanized GF. The flexural and impact properties of specimens were evaluated by means of three-point-bending tests and Charpy impact testing, respectively. The residual reactivity of the samples was analyzed using differential scanning calorimetry. The results of mechanical testing showed that acid and base pretreatments of the glass fabric had a positive effect on the flexural modulus of prepared composites but a negative effect on their impact strength. Possible interfacial adhesion mechanisms and the diffusion control of isothermal cure reactions due to vitrification have been discussed.
This paper investigates the casting defects of a stainless steel pump impeller manufactured through the sand casting process. The material characterization of austenitic steel AISI 316L was initially ...carried out, which examined the chemical composition of the casting and its microstructure. The next step was to determine the cause of the casting defects using numerical simulations. The numerical simulations were performed using ProCAST software (Version 18.0). Initial results of the filling and solidification simulations were conducted using the parameters employed in the actual casting process, revealing casting defects in corresponding locations. The casting process was subsequently modified to achieve improved results. This involved reconstructing the gating system, redesigning the riser, and incorporating a cylindrical chiller. The results show that the modified casting process significantly reduces the occurrence of defects in the final product. The study provides useful insights into the analysis and modification of the casting process for stainless steel pump impellers produced through sand casting. The results can help improve the quality of such products and reduce production costs associated with casting defects.
Laser-powder bed fusion (LPBF) is one of the preferred techniques for producing Co-Cr metal structures for dental prosthodontic appliances. However, there is generally insufficient information about ...material properties related to the production process and parameters. This study was conducted on samples produced from three different commercially available Co-Cr dental alloys produced on three different LPBF machines. Identically prepared samples were used for tensile, three-point bending, and toughness tests. Light microscopy (LM), scanning electron microscopy (SEM), and electron backscatter diffraction (EBSD) analyses of microstructure were performed after testing. Differences were observed in microstructures, which reflected statistically significant differences in mechanical properties (one-way analysis of variance (ANOVA) and Scheffé post hoc test (α = 0.05)). The material produced on the 3D Systems DMP Dental 100 had 24 times greater elongation ε than the material produced on the Sysma MySint 100 device and the EOS M100 machine. On the other hand, the material produced on the EOS M100 had significantly higher hardness (HV0.2) than the other two produced materials. However, the microstructure of the Sysma specimens with its morphology deviates considerably from the studied group. LPBF-prepared Co-Cr dental alloys demonstrated significant differences in their microstructures and, consequently, mechanical properties.
The anterolateral ligament is recently recognized as an important structure in restoring rotational stability of the anterior cruciate ligament-deficient knee. Biomechanical and clinical studies ...confirmed the benefits of concurrent anterior cruciate ligament and anterolateral ligament reconstruction. However, present techniques mostly use hamstring tendons autografts and therefore additionally disrupt the knee biomechanics. The plantaris tendon is a well known and accessible graft and has excellent biomechanical properties for anterolateral ligament reconstruction. The present paper describes a new combined anterior cruciate ligament and anterolateral ligament reconstruction technique using plantaris tendon and semitendinosus tendon.
Level of evidence
V (Case report).
To determine the shear bond strengths of different denture base resins to different types of prefabricated teeth (acrylic, nanohybrid composite, and cross-linked) and denture teeth produced by ...computer-aided design/computer-aided manufacturing (CAD/CAM) technology.
Prefabricated teeth and CAD/CAM (milled) denture teeth were divided into 10 groups and bonded to different denture base materials. Groups 1-3 comprised of different types of prefabricated teeth and cold-polymerized denture base resin; groups 4-6 comprised of different types of prefabricated teeth and heat-polymerized denture base resin; groups 7-9 comprised of different types of prefabricated teeth and CAD/CAM (milled) denture base resin; and group 10 comprised of milled denture teeth produced by CAD/CAM technology and CAD/CAM (milled) denture base resin. A universal testing machine was used to evaluate the shear bond strength for all specimens. One-way ANOVA and Tukey post-hoc test were used for analyzing the data (α=.05).
The shear bond strengths of different groups ranged from 3.37 ± 2.14 MPa to 18.10 ± 2.68 MPa. Statistical analysis showed significant differences among the tested groups (
<.0001). Among different polymerization methods, the lowest values were determined in cold-polymerized resin.There was no significant difference between the shear bond strength values of heat-polymerized and CAD/CAM (milled) denture base resins.
Different combinations of materials for removable denture base and denture teeth can affect their bond strength. Cold-polymerized resin should be avoided for attaching prefabricated teeth to a denture base. CAD/CAM (milled) and heat-polymerized denture base resins bonded to different types of prefabricated teeth show similar shear bond strength values.
This research investigates the impact of three process parameters of Laser Powder Bed Fusion (LPBF) - laser power, scanning speed, and base plate preheating temperature on the structure and ...mechanical properties of the EOS CoCr SP2 dental alloy. The LPBF process was used to fabricate dental Co–Cr alloy specimens for microstructural analysis and mechanical properties testing. Light and electron microscopy were used to determine microstructural parameters, including porosity, inclusions, and cracks. The material's chemical composition was analysed by EDS, while XRD and EBSD methods were used to determine the presence of microstructural phases and the crystallographic orientation of individual grains. The mechanical properties were evaluated through a static tensile test (Rp0.2, ε), a toughness test (KVa), and a three-point bending test to determine the flexural strength (Rms). In the microstructure, differences were observed that reflected statistically significant differences in mechanical properties (one-way analysis of variance (ANOVA) and Scheffé post hoc test (α = 0.05)) Using the base plate preheating temperature ϑp = 310 °C with a constant scanning speed v = 900 mm/s in combination with increasing laser power P from 160 W to 250 W the proportion of porosity decreased while the mechanical properties of toughness (KVa) and flexural strength (Rms) increase to maximum values.
The wear of induction cladded coating during motion was investigated through the abrasive mass at a speed of 1.0 to 3.0 m/s and the impact angle of abrasive particles with a worn surface of 0degrees ...to 90degrees. Cladding was performed by using Ni-Cr-Si-B-Fe flame spraying powder. Experimental research was carried out by using the Response Surface Method (RSM) and Central Composite Design (CCD). Analysis of variance proved that both motion speed and impact angle had significant impact on the wear of coating, both individually and interactively. Motion speed had the greatest influence, and the interaction of speed and angle had the least influence. The wear rate increased along with the motion speed increase, and the influence of the impact angle depends on the wear speed. At a speed of 1 m/s, the wear increases along with the increase of angle from 0degrees to 45degrees and then continues to decrease up to the angle of 90degrees. At a speed of 2 m/s, the wear increases along with the angle increase from 0degrees to 30degrees and then continues to decrease up to the angle of 90degrees. At a speed of 3 m/s, the wear increases along with the angle increase from 0degrees to 20degrees and then decreases as the angle increases up to 90degrees. Based on the statistical data processing, this research developed the mathematical model of wear in the form of quadratic polynomial that describes the influences of input variables in individual and interactive form.
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