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Maccato, Chiara; Bigiani, Lorenzo; Carraro, Giorgio; Gasparotto, Alberto; Seraglia, Roberta; Kim, Jiyeon; Devi, Anjana; Tabacchi, Gloria; Fois, Ettore; Pace, Giuseppe; Di Noto, Vito; Barreca, Davide
Chemistry : a European journal, 2017-Dec-19, 2017-12-19, Letnik: 23, Številka: 71Journal Article
Molecular engineering of manganese(II) diamine diketonate precursors is a key issue for their use in the vapor deposition of manganese oxide materials. Herein, two closely related β-diketonate diamine Mn adducts with different fluorine contents in the diketonate ligands are examined. The target compounds were synthesized by a simple procedure and, for the first time, thoroughly characterized by a joint experimental-theoretical approach, to understand the influence of the ligand on their structures, electronic properties, thermal behavior, and reactivity. The target compounds are monomeric and exhibit a pseudo-octahedral coordination of the Mn centers, with differences in their structure and fragmentation processes related to the ligand nature. Both complexes can be readily vaporized without premature side decompositions, a favorable feature for their use as precursors for chemical vapor deposition (CVD) or atomic layer deposition applications. Preliminary CVD experiments at moderate growth temperatures enabled the fabrication of high-purity, single-phase Mn O nanosystems with tailored morphology, which hold great promise for various technological applications.
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JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
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in: SICRIS
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