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Pointurier, Fabien; Williams, Ross W.; LaMont, Stephen P.; Steiner, Robert E.; Bostick, Debbie A.; Olsen, Khris B.; Wogman, Ned A.
Journal of radioanalytical and nuclear chemistry, 05/2013, Letnik: 296, Številka: 2Journal Article
In the framework of a collaboration between laboratories involved in bulk U and Pu analysis of environmental samples (DIF centre of the French Commissariat à l’Energie Atomique, US National Laboratories of New Brunswick, Lawrence Livermore, Pacific Northwest, Oak Ridge, and Los Alamos), two round-robins were organised, each one consisting of the complete analysis (chemical preparation and isotope measurement) of three Quality Control samples. The samples were 10 × 10 cm cotton tissues (“swipe samples”) containing low amounts of U (from ~20 to ~150 ng) and Pu (from ~0.15 to ~10 pg). Despite using different spikes, different methods of sample preparation and different analytical instrumentation, the results for U and Pu contents and isotopic compositions reported by all laboratories are globally in good agreement. All laboratories are able to measure sub-pg amounts of U and Pu isotopes with acceptable accuracy and reproducibility, even if limited discrepancies are observed affecting one or other measurement and/or laboratory. General and laboratory specific recommendations were discussed and adopted to continue to improve the accuracy and precision of the measurements.
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JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
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in: SICRIS
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