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Mao, Yuanbing; Wong, Stanislaus S
Journal of the American Chemical Society, 06/2006, Letnik: 128, Številka: 25Journal Article
A size- and shape-dependent morphological transformation was demonstrated during the hydrothermal soft chemical transformation, in neutral solution, of titanate nanostructures into their anatase titania counterparts. Specifically, lepidocrocite hydrogen titanate nanotubes with diameters of ∼10 nm were transformed into anatase nanoparticles with an average size of 12 nm. Lepidocrocite hydrogen titanate nanowires with relatively small diameters (average diameter range of ≤ 200 nm) were converted into single-crystalline anatase nanowires with relatively smooth surfaces. Larger diameter (>200 nm) titanate wires were transformed into analogous anatase submicron wire motifs, resembling clusters of adjoining anatase nanocrystals with perfectly parallel, oriented fringes. Our results indicate that as-synthesized TiO2 nanostructures possessed higher photocatalytic activity than the commercial titania precursors from whence they were derived.
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