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Sünkel, Karlheinz; Weigand, Stefan; Hoffmann, Alexander; Blomeyer, Sebastian; Reuter, Christian G; Vishnevskiy, Yury V; Mitzel, Norbert W
Journal of the American Chemical Society, 01/2015, Letnik: 137, Številka: 1Journal Article
Starting from ferrocene, pentafluoroferrocene Fe(C5F5)(C5H5) can be prepared in five steps via a one-pot lithiation–electrophilic fluorination strategy. Pentafluoroferrocene was characterized by multinuclear NMR and IR spectroscopy, by cyclovoltammetry as well as X-ray (solid) and electron diffraction (gas) and the experimental results compared with DFT calculations.
