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Sapchenko, Sergey A; Barsukova, Marina O; Belosludov, Rodion V; Kovalenko, Konstantin A; Samsonenko, Denis G; Poryvaev, Artem S; Sheveleva, Alena M; Fedin, Matvey V; Bogomyakov, Artem S; Dybtsev, Danil N; Schröder, Martin; Fedin, Vladimir P
Inorganic chemistry, 05/2019, Letnik: 58, Številka: 10Journal Article
Two new isostructural microporous coordination frameworks Mn3(Hpdc)2(pdc)2 (1) and Mg3(Hpdc)2(pdc)2 (2) (pdc2– = pyridine-2,4-dicarboxylate) showing primitive cubic (pcu) topology have been prepared and characterized. The pore aperture of the channels is too narrow for the efficient adsorption of N2; however, both compounds demonstrate substantially higher uptake of CO2 (119.9 mL·g–1 for 1 and 102.5 mL·g–1 for 2 at 195 K, 1 bar). Despite of their structural similarities, 2 shows a typical reversible type I isotherm for adsorption/desorption of CO2, while 1 features a two-step adsorption process with a very broad hysteresis between the adsorption and desorption curves. This behavior can be explained by a combination of density functional theory calculations, sorption, and X-ray diffraction analysis and gives insights into the further development of new sorbents showing adsorption/desorption hysteresis.
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