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Turchenko, V. A.; Trukhanov, S. V.; Kostishin, V. G.; Damay, F.; Porcher, F.; Klygach, D. S.; Vakhitov, M. G.; Lyakhov, D.; Michels, D.; Bozzo, B.; Fina, I.; Almessiere, M. A.; Slimani, Y.; Baykal, A.; Zhou, D.; Trukhanov, A. V.
Scientific reports, 09/2021, Letnik: 11, Številka: 1Journal Article
Abstract Indium-substituted strontium hexaferrites were prepared by the conventional solid-phase reaction method. Neutron diffraction patterns were obtained at room temperature and analyzed using the Rietveld methods. A linear dependence of the unit cell parameters is found. In 3+ cations are located mainly in octahedral positions of 4f VI and 12 k. The average crystallite size varies within 0.84–0.65 μm. With increasing substitution, the T C Curie temperature decreases monotonically down to ~ 520 K. ZFC and FC measurements showed a frustrated state. Upon substitution, the average and maximum sizes of ferrimagnetic clusters change in the opposite direction. The M r remanent magnetization decreases down to ~ 20.2 emu/g at room temperature. The M s spontaneous magnetization and the k eff effective magnetocrystalline anisotropy constant are determined. With increasing substitution, the maximum of the ε / real part of permittivity decreases in magnitude from ~ 3.3 to ~ 1.9 and shifts towards low frequencies from ~ 45.5 GHz to ~ 37.4 GHz. The maximum of the tg(α) dielectric loss tangent decreases from ~ 1.0 to ~ 0.7 and shifts towards low frequencies from ~ 40.6 GHz to ~ 37.3 GHz. The low-frequency maximum of the μ / real part of permeability decreases from ~ 1.8 to ~ 0.9 and slightly shifts towards high frequencies up to ~ 34.7 GHz. The maximum of the tg(δ) magnetic loss tangent decreases from ~ 0.7 to ~ 0.5 and shifts slightly towards low frequencies from ~ 40.5 GHz to ~ 37.7 GHz. The discussion of microwave properties is based on the saturation magnetization, natural ferromagnetic resonance and dielectric polarization types.
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