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Raziskave kovinskih mateialov z visoko ločljivim Augerjevim spektrometrom na poljsko emisijo : prve izkušnje = Investigations of metallic materials with high resolution field emission Auger Electron Spectrometer : first experiences
Jenko, Monika
Spektroskopijo Augerjevih elektronov, ki je najbolj razširjena analitska tehnika za raziskave strukture in sestave trdnih površin že skoraj tri desetletja s pridom uporabljajo tudi metalurgi in ...materialisti za raziskave površin čistih kovin in zlitin, za študij mehanizma in kinetike oksidnih plasti kovin in zlitin, za karakterizacijo anodno oksidiranih, pasivacijskih in korozijskih plasti, za raziskave ultra tankih segregiranih plasti na površinah, mejah zrn in faz ter vključkov. Namen prispevka je kratka predstavitev novega instrumenta Microlab 310-F, ki je dodatno opremljen z rentgenskim fotoelektronskim spektrometrom (XPS) in z lomilno napravo, ki omogoča prelom vzorcev v ultra visokem vakuumu (UVV) in študij fizikalno kemijskih procesov na mejah kristalnih zrn, faz in vključkov. Podan bo pregled letošnjih raziskav kovinskih materialov: karakterizacija izločkov, precipitatov in vključkov v jeklih ter v aluminiju in aluminijevih zlitinah, kot tudi raziskave čistih površin Ti, Gd, Er, Ir in Si.
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