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Carboxylic acid-tuned nickel(ii) clusters: syntheses, structures, solution behaviours and magnetic properties [Elektronski vir]Su, Yan-Min ...Three novel cicada-like nickel(II) clusters, formulated as [Ni6(bdped)2(mba)6(Hdmpz)2(NO3)2(H2O)2]· 4MeCN (SD/Ni6b), [Ni5(bdped)2(tca)6(Hdmpz)(MeOH)2(H2O)]·MeOH (SD/Ni5a) and [Ni4(Hbdped)2- ... (ba)4(Hdmpz)2]·2NO3·2MeCN (SD/Ni4a), were obtained by tuning the auxiliary carboxylic acids, where H2bdped = 1,2-bis-(3,5-dimethylpyrazol-1-yl)-ethane-1,2-diol; Hmba = 2-methylbenzoic acid; Hdmpz = 3,5-dimethyl-1H-pyrazole; Htca = 3-thiophenecarboxylic acid; and Hba = benzoic acid. The structures of SD/Ni6b, SD/Ni5a and SD/Ni4a are built from a central Ni4O4 opened cube, appending two to zero NiNO5 octahedra. The solution behaviours of SD/Ni6b, SD/Ni5a and SD/Ni4a were studied in detail via an ESI-MS technique and their solution stabilities were confirmed. Magnetic analysis indicated the presence of Ising-type anisotropy: D = −13, −10, and −11 cm−1 for SD/Ni6b, SD/Ni5a, and SD/Ni4a, respectively; moreover, dominantly ferromagnetic interactions were found between magnetic centers: J1 = 6.5 cm−1 , J2 = −0.44 cm−1 and J1 = 5.9 cm−1 , J2 = 2.6 cm−1 for SD/Ni5a and SD/Ni4a, respectively. Besides, the photocurrent signals were observed and they reached the maximum very quickly for these three nickel(II) clusters and then their current intensities remained almost constant, which provide a possibility to be used for light-harvesting and photo-related catalysis.Source: Dalton transactions [Elektronski vir]. - ISSN 1477-9234 (Vol. 50, iss. 12, March 2021, 4355-4362)Type of material - e-article ; adult, seriousPublish date - 2021Language - englishCOBISS.SI-ID - 126564099
Author
Su, Yan-Min |
Ji, Bao-Qian |
Shao, Feng |
Zhang, Shan-Shan |
Jagodič, Marko, 1981- |
Jagličić, Zvonko |
Gao, Zhi-Yong |
Dou, Jian-Min |
Sun, Di
Topics
Ni(II) kompleks |
struktura |
magnetne lastnosti |
nickel(II) clusters |
structure |
magnetic properties
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Database name | Field | Year |
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Links to authors' personal bibliographies | Links to information on researchers in the SICRIS system |
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Su, Yan-Min | |
Ji, Bao-Qian | |
Shao, Feng | |
Zhang, Shan-Shan | |
Jagodič, Marko, 1981- | 28581 |
Jagličić, Zvonko | 11892 |
Gao, Zhi-Yong | |
Dou, Jian-Min | |
Sun, Di |
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