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Application of surface analytical technique HRAES to metallurgy
Jenko, Monika ; Mandrino, Djordje
Kakovost razžveplanih kontinuirno ulitih jeklenih gredij je zelo odvisna od vsebnosti, razporeditve in kemijske sestave vključkov. Z Augerjevo spektroskopijo elektronov visoke ločljivosti so ...preiskani vključki v jeklu z 0,035% masnega deleža žvepla in 0,20 do 0,40% masnega deleža aluminija. Prvič v proizvodnji jekla je prikazana kemijska sestava in razporeditev Ca, S in O v vključkih. S pomočjo HRAES je bila opravljena analiza količine Cr, Mo in V precipitatov v jeklu XCr12MoV. Velikost precipitatov je med 10 in 60 nm. Pri žarjenju na 800°C je najdena karbidna faza molne sestave ▫$M_3C_2$▫ s kromom in železom kot kationi, z ogljikom in dušikom kot anioni, medtem ko je po žarjenju pri 650°C najdeni karbid ▫$M_{23}4C_6$▫ s kromom, molibdenom in železom kot kationi.
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