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Postopek za sintezo 2-n-oktil-4-izotiazolin-3-ona : patent št.: 9500241
Bauman, Davorin ...
Opisan je nov, tehnološko napreden postopek za sintezo 2-n-oktil-4-izotiazolin-3-ona, ki daje visoke dobitke. 2-n-oktil-4izotiazolin-3-on pripravimo izhajajoč iz n-oktil merkaptopropion amida ...dobljenega z amidacijo metilnega estra merkaptopropionske kisline z n-oktilom aminom pri tlakih med 30 in 250 bar. Ciklizacija amida merkaptopropionske kisline v 2-n-oktil-4-izotiazolin-3-on poteka oksidativno ob uvajanju klora pri tlakih med 30 in 350 bar.
Type of material - patent
Publication and manufacture - Ljubljana : Urad RS za intelektualno lastnino, 28.2.1997
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