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Synthesis and structure determination of a chain-like aluminophosphate obtained with 1,2-diaminopropane as the structure-directing agentRajić, Nevenka ...Colorless plate-like crystals (AlPO-1,2DAP) crystallize from a clear `AlPO4-1,2-diaminopropaneć reaction system. The results of elemental, thermal and FTIR analyses give the following chemical ... formulaČ (NH4+)(1,2-H2DAP)2+(AlP2O8)3-, confirmed also by single crystal structure determination. The X-ray diffraction data collected at 150 K reveal the space group Pc21n with a=8.2788(2), b=16.7882(3), c=8.6608(2) Å, and V=1203.73(5) Å3. The AlPO-1,2DAP has a chain structure related to the aluminophosphate AlPO-enA structure. Two occluded cations, NH4+ and doubly protonated diamine, balance the negative charge and interact with the chain oxygen atoms via hydrogen bond network.Source: The Journal of physics and chemistry of solids. - ISSN 0022-3697 (Vol. 64, no. 7, 2003, str. 1097-1103)Type of material - article, component partPublish date - 2003Language - englishCOBISS.SI-ID - 2814234
Author
Rajić, Nevenka |
Zabukovec Logar, Nataša |
Golobič, Amalija |
Kaučič, Venčeslav
Topics
strukturna kemija |
kristalografija |
koordinacijske spojine |
kristalna struktura |
rentgenska difrakcija |
določitev strukture spojin |
anorgansko organski hibridi |
aluminijeve spojine |
aluminijevi fosfati |
aluminij |
inorganic organic hybrid |
aluminophosphate |
porous materials synthesis |
crystal structure |
X-ray diffraction
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Database name | Field | Year |
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Links to authors' personal bibliographies | Links to information on researchers in the SICRIS system |
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Rajić, Nevenka | 10664 |
Zabukovec Logar, Nataša | 14120 |
Golobič, Amalija | 12624 |
Kaučič, Venčeslav | 03373 |
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