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IL-SEM : primer študije elektrokemijske degradacije zlitine nanodelcev PtNi
Hodnik, Nejc, dipl. kemik ...
Elektrokemijska degradacija zlitine nanodelcev PtNi je bila študirana z novo nedestruktivno metodo, ki smo jo poimenovali identična lokacija vrstične elektronske mikroskopije (identical location ...scanning electron microscopy, IL- SEM), S to metodo je omogočeno opazovanje na istem mestu (na istem nanodelcu) pred in po elektrokemijski obdelavi. Študija je bila dopolnjena še z drugimi metodami, kot so rentgenska praškovna difrakcija, XRD in elektrokemijska meritev z disk elektrodo. Po začetnem potencialnem ciklanju rezultati kažejo, da prihaja do raztapljanja Ni iz zlitine PtNi in s tem do povečanja elektrokemijske površine (electrochemical surface area, ESA). Po pospešenem degradacijskem testu (accelerated degradation test, ADT) se morfologija opazno spremeni (SEM slika). Pojavi se hrapavost na površini nanodelcev, hkrati pa se zmanjša aktivnost za reakcijo redukcije kisika.
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