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Synthesis and use of ortho-(branched alkoxy)-tert-butoxybenzenesRast, Slavko ; Stephan, Michel ; Mohar, BarbaraA series of sterically hindered o-(branched alkoxy)-tert-butoxybenzenes was efficiently prepared in good yields owing to a new practical and simple preparation of o-tert-butoxyphenol starting from ... catechol and isobutene. Use of DMF di-tert-butyl acetal reagent instead of isobutene/H2SO4 (cat.) for O-tert-butylation was very convenient in case of ortho bulky phenols affording the corresponding tert-butyl ethers in high yield and purity. This general route proved to be useful since no reliable access was available to o-di-t-BuO-substituted arenes. Application to the synthesis of congested phosphorus-based compounds is presented.Source: Tetrahedron letters. - ISSN 0040-4039 (Vol. 53, no. 50, 2012, str. 6815-6818)Type of material - article, component partPublish date - 2012Language - englishCOBISS.SI-ID - 5119258
Author
Rast, Slavko |
Stephan, Michel |
Mohar, Barbara
Topics
kemijska struktura |
sinteza snovi |
tehnologija |
uporaba
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Database name | Field | Year |
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Links to authors' personal bibliographies | Links to information on researchers in the SICRIS system |
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Rast, Slavko | 33237 |
Stephan, Michel | 25361 |
Mohar, Barbara | 12832 |
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