-
Simultaneous analysis of ascorbic and dehydroascorbic acid in fruit juice using HILIC chromatography coupled with mass spectrometryZia, Hassan ...A HILIC-MS/MS method was developed for the simultaneous analysis of ascorbic acid (AA) and dehydroascorbic acid (DHA). Ammonium acetate buffer and acetonitrile were used as mobile phases under ... gradient elution mode at a flow rate of 0.3 mL/min. A SCIEX Triple QUAD 5500+ system was operated under MRM mode to acquire data with 175 → 115 and 173→113 as the quantifier ions for AA and DHA, respectively. Samples were prepared with a simple dilute and shoot method. A calibration and accuracy study was performed as part of method validation in fruit juices. The accuracy profiles were estimated from the measurement uncertainty determined from the validation data according to the ISO/DTS 21748. The recoveries of the analytes were between 92 – 130 %. The LOQs achieved in the current study for AA and DHA were 4.5 μg/L and 18 μg/L, respectively. These LOQs were substantially lower than what has been previously reported in the literature. The study concludes with a straightforward analytical method for the determination of total vitamin C content that does not involve timing consuming steps i.e., reduction or derivatization reaction. The method can be implemented in quality control labs for routine analysis of food samples.Vir: Journal of food composition and analysis. - ISSN 0889-1575 (Vol. 124, art. no. 105714, 2023, 7 str.)Vrsta gradiva - članek, sestavni delLeto - 2023Jezik - angleškiCOBISS.SI-ID - 169061379
Avtor
Zia, Hassan |
Fischbach, Nadine |
Hofsommer, Mikko |
Slatnar, Ana
Teme
HPLC-MS/MS |
quality control |
multifruit juice |
fruit juices |
ascorbic acid |
dehydroascorbic acid |
accuracy profile |
validation |
sadni sok |
vitamini |
askorbinska kislina |
dehidroaskorbinska kislina |
kemična sestava |
HPLC-MS/MS |
kakovost
Avtor | Zia, Hassan ... |
Naslov | Simultaneous analysis of ascorbic and dehydroascorbic acid in fruit juice using HILIC chromatography coupled with mass spectrometry |
Datum objave | 2023-09-25 |
COBISS.SI-ID | 169061379 |
Verzija objave v repozitoriju | Založnikova različica |
Licenca objave v repozitoriju | Creative Commons Priznanje avtorstva-Nekomercialno-Brez predelav 4.0 Mednarodna |
Embargo | Takojšnja javna objava |
Projekti, iz katerih je bila financirana objava
Naziv | Akronim | Številka projekta | Financer |
---|---|---|---|
Establishing a strong and lasting international training network for innovation in food and juice industries: a 4D-research approach for fruit juice processing | HiStabJuice | 956257 |
European Commission |
Datoteke, ki spadajo k objavi
Povezava |
---|
https://www.sciencedirect.com/science/article/pii/S0889157523005884 |
https://repozitorij.uni-lj.si/IzpisGradiva.php?id=151767 |
Vnos na polico
Trajna povezava
- URL:
Faktor vpliva
Dostop do baze podatkov JCR je dovoljen samo uporabnikom iz Slovenije. Vaš trenutni IP-naslov ni na seznamu dovoljenih za dostop, zato je potrebna avtentikacija z ustreznim računom AAI.
Leto | Faktor vpliva | Izdaja | Kategorija | Razvrstitev | ||||
---|---|---|---|---|---|---|---|---|
JCR | SNIP | JCR | SNIP | JCR | SNIP | JCR | SNIP |
Baze podatkov, v katerih je revija indeksirana
Ime baze podatkov | Področje | Leto |
---|
Povezave do osebnih bibliografij avtorjev | Povezave do podatkov o raziskovalcih v sistemu SICRIS |
---|---|
Zia, Hassan | |
Fischbach, Nadine | |
Hofsommer, Mikko | |
Slatnar, Ana | 30707 |
Izberite prevzemno mesto:
Prevzem gradiva po pošti
Obvestilo
Gesla v Splošnem geslovniku COBISS
Izbira mesta prevzema
Mesto prevzema | Status gradiva | Rezervacija |
---|
Prosimo, počakajte trenutek.